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Deep Reactive Ion Etching (DRIE)

To create deep, steep-sided holes and trenches in wafers/substrates

PlasmaPro 100 Estrelas DRIE

Designed to give total flexibility for Deep Reactive Ion Etching (DRIE) applications


Deep Reactive Ion Etching (DRIE)


Designed to enable the fabrication of all Si etch devices, Deep Silicon Etching delivers:

  • Process Flexibility​
  • High etch rates​
  • High selectivity to photoresist (PR) and oxide​
  • High Aspect-ratio​
  • Smooth sidewalls​
  • Minimised mask undercut​
  • SOI capability​
  • Si thinning & high Si exposed​
  • Capable SiO2 etch


DSiE Overview


Deep Reactive Ion etching of Silicon (DRIE), or Deep Silicon Etching (DSiE), is a highly anisotropic etch process used to create deep, steep-sided holes and trenches in wafers/substrates, typically with high aspect ratios.

The Estrelas® DSiE system offers ultimate process flexibility, serving multiple process solutions across the Micro Electro Mechanical Systems (MEMS), Advanced Packaging and Nanotechnology markets.



DSiE processes


The two technologies used to achieve deep etches in the fabrication of micro-electro-mechanical systems (MEMS) are the Bosch and the Cryogenic Processes. System and process development over many years has allowed the techniques to advance but the fundamental aspects of each remain the same:

  • Bosch process enables high etch rates, selectivity and anisotropy, and is typically used for features >1µm and depths >10µm​
  • Cryogenic Deep Silicon Etch (Cryo-DSiE) is typically used for smooth sidewalls and/or nano-etching or tapered profiles in applications such as micro moulds etc.
  • Mixed processes are an option for shallow, low aspect fine features.
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Bosch process


Typical applications include MEMS, Microfluidics and Medical

The Bosch process uses a fluorine based plasma chemistry to etch the silicon, combined with a fluorocarbon plasma process to provide sidewall passivation and improved selectivity to etch mask. A complete etch process cycles between etch and deposition steps many times to achieve deep, vertical etch profiles. It relies on the source gases being broken down in a high-density plasma region before reaching the wafer.

This technique cannot be performed in reactive ion etch systems (RIE), as these have the wrong balance of ions to free radical species. This balance can be achieved in high-density plasma systems (HDP). The most widely used form of HDP uses inductive coupling to generate the high-density plasma region so is known as ‘inductively coupled plasma’ (ICP).


DSiE Bosch Process Stages


High rate, controlled scallops e.g. Microfluidics (200 µm depth), vias (> 400 µm depth)

High rate, controlled scallops e.g. Microfluidics (200 µm depth), vias (> 400 µm depth)

Microneedles created using the Bosch process ​

Microneedles created using the Bosch process ​

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Cryo process


Typical applications include MEMS, Photonics and Biomedical

Just as for the Bosch process, this technique also uses SF6 to provide fluorine radicals for silicon etching. The silicon is removed in the form of SiF4, which is volatile.

The main difference is in the mechanism of sidewall passivation and mask protection. Rather than using a fluorocarbon polymer, this process relies on forming a blocking layer of oxide/fluoride (SiOxFy) on the sidewalls (around 10-20nm thick), this forms at the cryogenic temperatures used and the layer inhibits the attack on the underlying Si layer by the fluorine radicals.

The low temperature and low bias operation also assists in reducing the etch rate of the mask material, which is normally either photoresist or silicon dioxide.


Micro-mould created using the Cryo process

Si waveguide etch

Smooth sidewall cryogenic DSE (no scallops).
Courtesy TU Twente

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Featured DRiE products



PlasmaPro 100 Estrelas DRIE


The PlasmaPro 100 Estrelas platform is designed to give total flexibility for Deep Reactive Ion Etching (DRIE) applications - serving a diverse set of process requirements across the Micro Electromechanical Systems (MEMS), Advanced Packaging and Nanotechnology markets. Developed for research and volume production, the PlasmaPro 100 Estrelas offers the ultimate flexibility with Bosch and Cryogenic processes.

  • High etch rate and high selectivity with Bosch process
  • Smooth sidewall & high aspect ratio processes
  • Highly anisotropic (vertical) profile
  • Low rate, low power for nano-silicon etch and notch control (SOI)
  • Tapered via etches
  • Wide range of applications
  • Mechanical or electrostatic clamping (substrates’ compatibility)
  • Improved reproducibility
  • Increased mean time between cleans (MTBC)


Overview of PlasmaPro 100 Estrelas DRIE


DSiE technique or Deep Reactive Ion Etching (DRIE) combines isotropic silicon etching and passivation steps repeatedly to obtain anisotropic profiles. Using high density plasma source and fast gas-switching capability, this technique enables you to achieve profile verticality, smooth sidewalls and high etching rates with high selectivity to masking materials.

From smooth sidewall processes to high rate cavity etches and high aspect ratio processes to tapered via etches, the PlasmaPro 100 Estrelas has been designed to ensure that the wide range of applications in MEMS, advanced packaging and nanotechnology can be realised without the need to change chamber hardware.

Nano and microstructures can be realised as the hardware has been designed with the ability to run Bosch™ and Cryo etch technologies in the same chamber.



Features of PlasmaPro 100 Estrelas DRIE


  • Compatible with 50mm to 200mm substrates - ensures you have the ability to develop devices that can be taken to production using the same chamber hardware
  • Auto match - Process flexibility
  • Higher flow MFCs and associated generators - High radical densities
  • Reduced chamber volume and high throughput pumping - Ensures high gas conductance
  • Fast-acting close-coupled MFCs - Fast control (originally developed for ALD)

System requirements

  • High-density plasma (chemically-driven process)
  • Close-coupled gas pod
  • High flow and pumping
  • Fast and easy switching easy from liquid nitrogen (LN2) to the chiller and vice-versa
  • Advanced recipe editor
  • Heated liners and top plate
  • Efficient wafer cooling


Applications for PlasmaPro 100 Estrelas DRIE


Bosch applications

  • MEMS for Smart Devices, Consumer & Industrial Electronics
  • Microfluids
  • Biomedical Devices​
  • Through Silicon Via (TSV)
  • SiO2 and Quartz Etch
  • High Q Capacitor Arrays and High Q Resonators for Quantum Devices

Cryo applications

Cryogenic DSiE is typically used for smooth sidewalls and/or nano-etching and temperature sensitive materials, as it provides low temperature process (» -110°C)

  • Nano Applications
  • Photonics
  • Moulding


Specifications for PlasmaPro 100 Estrelas DRIE


Parameter

Bosch

Cryogenic

Mixed gas

Rate (μm/min)

High

Moderate

Low

Selectivity to PR

Very high

High

Low

Profile

Vertical

Vertical or Sloped

Vertical or Sloped

Aspect ratio

Very high

High

Low

Sidewalls

Scallops

Smooth

Smooth

ARDE control

Yes

Limited

Limited

Cleaning

Regular

Rare

Regular

Min. feature /nm

≈ 300

≈ 10

30


Global customer support

Oxford Instruments is committed to providing a comprehensive, flexible and reliable global customer support. We offer excellent quality service throughout the life of your system.

  • Remote diagnostics software provides quick and easy fault diagnosis and resolution.
  • Support contracts are available to suit the budget and situation.
  • Global spares in strategic locations for quick response.
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NEW: PTIQ software

PTIQ is the latest intelligent software solution for PlasmaPro and Ionfab processing equipment.

  • Exceptional level of responsive system control
  • Optimise system and process performance
  • Different levels of software to suit your requirements
  • Brand new intuitive layout and design
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Explore our comprehensive Training Training courses

At Oxford Instruments Plasma Technology, we offer a wide range of technical training courses designed to suit all skill levels and needs.

  • Level 1 (Introductory): New system users for all platforms
  • Level 2 (Intermediate): Equipment and maintenance training for all platforms
  • Level 3 (Advanced): for Plasma, Ion Beam and ALD systems
  • Specialist Technical Modules: process and handler technical training for all platforms
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Upgrades/Accessories

Gas pod - incorporate extra gas lines and allow greater flexibility

Logviewer software - datalogging software allows realtime graphing and post run analysis

Optical end point detectors - an important tool for achieving optimal process results

Soft pump - allows the slow pumping down of a vacuum chamber

Turbomolecular vacuum pump - offers superior pumping speeds and higher throughput

X20 Control System - delivers a future proof, flexible and reliable tool with increased system ‘intellect’

Advanced Energy Paramount generator - Offering increased reliability and greater plasma stability

Automatic pressure control - This controller ensures very fast and accurate pressure control

Dual CM gauge switching - provides the ability to utilise two differing ranges of capacitance manometer via a single pressure control valve

LN2 autochangeover unit - enables table cooling fluid to be automatically switched between Liquid Nitrogen (LN2) and Chiller Fluid

Wide temperature range electrode - significant design improvements to increase process performance

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